General

Content
NMR Bibliography

Proton NMR (HMR)

5.00 - NMR experiment, PDF
5.01 - Integration
5.02 - Chemical Shifts (δ)

Calculation
Shift effects
Anisotropy, Aromatic, ASIS
OH, NH, SH, SeH, TeH, FH

5.03 - Coupling (J), PDF
5.04 - Geminal J
5.05 - Vicinal J

Karplus Equation
Ring stereochem: 6, 5, 4, 3
Acyclic stereochem
Allylic
Olefin stereochem

5.06 - Long-range J

W-coupling
Allylic, Benzylic
Arom meta/para
Homoallylic
Alkynes, Allenes

5.07 - Spin nomenclature, PDF
5.08 - NMR symmetry
5.09 - Second order
5.10 - AX and AB
5.11 - AX₂ and AB₂
5.12 - ABX,

AMX, ABX
Solving ABX
5-LineABX
Typesof ABX
ABXYZ

5.13 - ABX₃
5.14 - A₂B₂
5.15 - AA'BB'
5.16 - Virtual coupling

H-NMR Data (HDATA)

9.1 - Proton shifts

9.4 - NMR solvents
9.5 - Shift calculations sp³
9.6 - Shift calculations sp²

9.7 - J(H-H) data

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Carbon NMR (CMR)

6.1 - Spectra,
6.2 - Chemical Shifts
6.3 - sp³ Carbons
6.4 - sp² Carbons
6.5 - One-bond J(CH)
6.6 - Two, three-bond J(CH)
6.7 - Long-range J(CH)
6.8 - Assignment

Carbon Data (CDATA)

10.4 - C-13 Shift data

10.5 - J(C-H) data

10.6 - J(C-C) data

Multinuclear NMR

7.1 - Nuclear properties

Summary
Fundamentals

7.2 - Effects on H, C NMR

100% Spin 1/2 Nuclei
Low Abundance Spin 1/2 Nuclei
Size of J for Spin 1/2 Nuclei
Second Order Effects
Coupling with Quadrupolar Nuclei
Deuteration
Effects of Boron
Effects of Nitrogen (in progress)
Isotope Shifts

7.3 - Other Spin 1/2 Nuclei

100% Spin 1/2Nuclei
Low Abundance Spin 1/2 Nuclei
Isotope Shifts
Relaxation

7.4 - Quadrupolar nuclei

Fundamentals -Symmetry
Summary

11.1 - NMR Nuclei:

Main group
Transition metals
Actinides

11.2 - Shift and J data

¹⁹F Chemical Shift

¹⁹F Coupling

³¹P Chemical Shift

³¹P Coupling

⁷⁷Se Chemical Shift

B-11

Topics in NMR

8.1 - Relaxation

T₁, T₂
SR, CSA, QR, SC, DD

8.2 - NOE
8.3 - DNMR

Temperature measurement
Thermodynamic parameters
Single bond rotation
Double bond rotation
Inversion
Double bond shift
Ligand exchange

8.4 - Saturation Transfer
8.5 - Saunders Isotope Shifts
8.7 - Shift reagents
8.9 - Multipulse NMR - 2D

NMR Data

NMR Solvents
NMR Acronyms
NMR Periodic Table

Exams, Problems

Exam 1 (2010), Answer
Exam 1 (2011), Answer
Exam 1 (2012), Answer
Exam 2 (2010), Answer
Exam 2 (2011), Answer
Exam 2 (2012), Answer
Exam 2 (2013), Answer
Exam 3 (2010), Answer
Exam 3 (2012), Answer
Exam 3 (2013), Answer
Problem Set 1, Answer
Problem Set 2, Answer
Problem Set 5, Answer
Problem Set 7, Answer
Problem Set 8 answer (partial)
Problem Set 9, Answer
Problem Set 10 (2014) Answer
Problem Set 11, Answer (partial)
Problem Set 11 (2014) Answer
Problem Set 12 (2013) Answer
Problem Set 12 (2014) Answer
Problem Set 13 (2013), Answer
Problem Set 13 (2014) Answer

Other Spectra Exercises

James Nowick, UC Irvine
Craig Merlic, UCLA
BradleySmith, Notre Dame