
Total synthesis of Ipsdienol (Sakurai):
Reference: | Hosomi, A.; Araki, Y.; Sakurai, H. J. Org. Chem. 1983, 48, 3122. DOI |
Reactions: | Si-Allyl+Aldehyde • Aldehyde+Si-R • O-SiMe3 → O-H • |
Reagents: | Allyl-SiR3 • Fluoride, R4N+ • HCl, MeOH • Fluoride, R4N+ • HCl, MeOH • |